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sublimation experiment... interpreting results?

This is probably a pretty basic question, but I am really confused on how to interpret the results of a sublimation experiment.

I tested samples of solid CaCO3, solid NH4Cl, and a mixture of the two by 1) heating the mixture and collected sublimed solids on a watch glass, and 2) by adding HCI to unheated samples of those two separate solids and a mixture of both and observing the reactions. 3) I then tested the collected solid from the first heated sample by adding HCI to it and observed the reaction as well.

Okay, no problem, I followed the directions, and observed the reactions. but I have NO CLUE how to interpret the data to identify what the collected solid is.

I'm not looking for the answer, because if I can't figure it out then I'm not learning anything in the process. But what do I need to compare? I'm looking at how the solid samples reacted with HCI, how the mixture reacted with HCI, and how the recovered solid reacted. I know one of the substances sublimed (went from solid to gas) when heated, but how do I go about figuring this out?

Any help would be GREATLY appreciated. I've got my first lab practical today and I need to understand this!

Update:

Thank you so much, Colin. That is what I was leaning towards, and I think you've confirmed it for me. Based on the reactions that I observed, I thought the NH4Cl was what had sublimed (and that the observable data from the mixture was the CaCO3 reacting). I really appreciate your help!

2 Answers

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  • Colin
    Lv 7
    1 decade ago
    Favorite Answer

    well, you clearly know NH4Cl sublimes and in part 1] if it is present in a mixture will do so as well

    in part 2] by adding HCl [conc or dilute?] you should be converting the samples to their chlorides .. do they sublime? presumably you got results in 2 of the 2 experiments here. CaCl2 doesn't sublime.

    part 3] you presumably collected the sublimate? NH4CL ... and then added HCl and heated again .. once HCl has boiled off, then you are heating NH4Cl

    Hope that is some help!

    Source(s): retired chemistry examiner
  • 5 years ago

    I think you need not worry if the mark wasnt near the answer area........i mean only if there is some mark in that area it can affect the checking.......even I gave my MCQ today! Good Luck

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