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How to make 2-octyl cyanoacrylate?
How do i go about making 2-octyl cyanoacrylate, i have searched and searched but i cant find a website that gives what steps i need to take in order to make it.
3 Answers
- GlenguinLv 71 decade agoFavorite Answer
The general method to make cyanoacrylates (Superglue) is by oxidation/elimination of an aryl selenyl group from the α-selenoaryl-α-cyanopropionate ester with hydrogen peroxide in chloroform:
CH3C(CN)(SeAr)CO2R → CH2=C(CN)CO2R
The patent below gives some guidance.
Source(s): US Patent 5504252 (Locktite Corp.)